Search results for "High-pressure synthesis"

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High-pressure synthesis of boron-rich chalcogenides B12S and B12Se

2022

The authors thank Drs. I. Dovgaliuk and T. Chauveau for assistance with Rietveld analysis; and Drs. V. Bushlya and A. Jamali for help with EDX/SEM measurements. This work was financially supported by the European Union's Horizon 2020 Research and Innovation Program under Flintstone2020 project (grant agreement No 689279).

Materials sciencePhononFOS: Physical scienceschemistry.chemical_element02 engineering and technologyCrystal structure[CHIM.INOR]Chemical Sciences/Inorganic chemistry01 natural sciencessymbols.namesake0103 physical sciences[CHIM.CRIS]Chemical Sciences/CristallographyMaterials ChemistryIsostructural010306 general physicsBoronCondensed Matter - Materials ScienceRietveld refinementMechanical EngineeringCrystal structureMetals and AlloysMaterials Science (cond-mat.mtrl-sci):NATURAL SCIENCES::Physics [Research Subject Categories][CHIM.MATE]Chemical Sciences/Material chemistry540021001 nanoscience & nanotechnologyCrystallographychemistryMechanics of MaterialsElemental analysisBoron-rich chalcogenidesddc:540symbolsRaman spectraHigh-pressure synthesis0210 nano-technologyRaman spectroscopyStoichiometry
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Magnetoelectric coupling driven by inverse magnetostriction in multiferroic BiMn3Mn4O12

2013

By means of neutron powder diffraction, we investigated the effect of the polar Bi$^{3+}$ ion on the magnetic ordering of the Mn$^{3+}$ ions in BiMn$_3$Mn$_4$O$_{12}$, the counterpart with \textit{quadruple} perovskite structure of the \textit{simple} perovskite BiMnO$_3$. The data are consistent with a \textit{noncentrosymmetric} spacegroup $Im$ which contrasts the \textit{centrosymmetric} one $I2/m$ previously reported for the isovalent and isomorphic compound LaMn$_3$Mn$_4$O$_{12}$, which gives evidence of a Bi$^{3+}$-induced polarization of the lattice. At low temperature, the two Mn$^{3+}$ sublattices of the $A'$ and $B$ sites order antiferromagnetically (AFM) in an independent manner …

Neutron powder diffractionMAGNETIC-STRUCTURESPEROVSKITEGeneral Physics and AstronomyDefect free02 engineering and technologyDIFFRACTION01 natural sciencesIonLattice (order)BIMNO30103 physical sciencesMultiferroicsCRYSTAL-STRUCTURE010306 general physicsPerovskite (structure)PhysicsAtomic force microscopy021001 nanoscience & nanotechnologyPOLYMORPHISMCrystallographyROOM-TEMPERATUREPolarHIGH-PRESSURE SYNTHESISBIMN7O12[PHYS.COND.CM-SCE]Physics [physics]/Condensed Matter [cond-mat]/Strongly Correlated Electrons [cond-mat.str-el]0210 nano-technologyTRANSITION
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